Microscopy lab providers with MicroVision Laboratories 2021
Sem/eds analysis providers in Chelmsford right now? As indicated in the FTIR spectral comparison below, the suspect material showed a near perfect match for acetylsalicylic acid. Additionally, there was a small amount of dibasic phosphate present. It was determined that the material was likely acetylsalicylic acid with a phosphate binder – an aspirin. Therefore, from this analysis the suspect material in the bottle was likely a household aspirin tablet, broken apart and separated by the water. In order to confirm the identification, a few aspirin tablets from several common manufacturers were obtained, roughly ground, and soaked to allow for comparison. The optical morphology of the crystals, size range of the particles, association with the phosphate and FTIR spectrum all were consistent with the original suspect material. A report detailing the methods and findings in full narrative form was rendered to the client.
In Fourier Transform Infrared (FTIR) Spectroscopy samples are subjected to a broad frequency spectrum of infrared light which spans the energies of intramolecular vibrations, especially in organic compounds. The pattern and intensity of frequencies absorbed by a sample are plotted, which gives structural information about the chemical bonding state of the material. Organic compounds, which are generally very similar from an elemental standpoint, can be separated and identified using these structural fingerprints.
What is your standard turnaround time (TAT) and can it be expedited? Our standard TAT is 5 to 10 business days. We can provide faster TATs on request with the following surcharges: – Same day to 24 hour rush is 100% surcharge – 2 day rush is 75% surcharge – 3 day rush is 50% surcharge – 4 day rush is 25% surcharge Rush requests must have prior approval otherwise we cannot guarantee turnaround times. Discover more details on go. We partner with companies in all phases of product development and sales, including R&D, manufacturing, QC, advertising and failure analysis. Our laboratory offers a highly-trained and experienced staff utilizing a powerful set of analytical tools (SEM with EDS and backscatter detectors, Bruker X-Flash elemental mapping, X-Ray imaging, Micro-FTIR spectroscopy, Micro-XRF, light microscopy, cross sectioning/precision polishing and microhardness testing).
An affected floor tile was submitted to determine if the previous mold testing had missed a source on the tile backing or mastic. Additionally, a new tile from the same manufacturing lot was submitted for comparison. The process of preparing and examining the sample and reference tile was documented. Areas with darkened surface features were imaged and then cut out and examined. While the dark spots looked very discrete when examined by eye, under top light polarized microscopy they appeared more diffuse at the outer edges. The darkest areas surrounded what appeared to be particles embedded in the surface.
MicroVision Laboratories’ analytical experts were able to meet with the QC Engineers and develop an analytical plan as to which solder joints to cross section and inspect. The client not only wanted to determine if there were any significant issues with the solder joint but also determine that there was a good intermetallic bond between the tin/lead solder and the copper wires of the chip packages. Explore extra details on here.
